3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate)

Base Information

Chemical Name:3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate)
CAS No.:324041-18-1
Molecular Formula:C₃₂H₃₀O₁₀
Molecular Weight:574.584
Hs Code.:

Synonyms:3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate)

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Technology Process of 3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate)

There total 4 articles about 3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13242-53-0
acetobromomannose

: 324041-18-1
3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate)

Guidance literature:: Multi-step reaction with 3 steps

1: 2,4-lutidine; molecular sieves 4 Angstroem / CH₂Cl₂

2: NaOH; MeOH

3: pyridine

With pyridine; methanol; sodium hydroxide; 2,4-lutidine; 4 A molecular sieve; In dichloromethane; 2: Zemplen deacetylation;
DOI:10.1055/s-2001-16062

Reference yield:

: 55864-95-4,136944-74-6
3,4,6-tri-O-acetyl-1,2-O-(allyloxyethylidene)-β-D-mannopyranose

: 324041-18-1
3,4,6-tri-O-benzoyl-α-D-mannopyranose 1,2-(allyl orthoacetate)

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol / 20 °C

2: pyridine

With sodium methylate; In pyridine; methanol;
DOI:10.1081/SCC-120003613