2-phenylthiopyridine nitroxide

Base Information

• Chemical Name: 2-phenylthiopyridine nitroxide
• CAS No.: 39574-22-6
• Molecular Formula: C₁₁H₉NOS
• Molecular Weight: 203.265
• Mol file: 39574-22-6.mol

Synonyms:2-phenylthiopyridine nitroxide

Chemical Property of 2-phenylthiopyridine nitroxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-phenylthiopyridine nitroxide

There total 7 articles about 2-phenylthiopyridine nitroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Cu(2-thio-pyridine N-oxide)2 + iodobenzene (591-50-4) → 2-phenylthiopyridine nitroxide (39574-22-6)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 80 - 100 ℃; for 9h; Wavelength;

DOI:10.1016/j.mcat.2021.111981

Reference yield: 60.0%

Cu(2-thio-pyridine N-oxide)2 + bromobenzene (108-86-1,52753-63-6) → 2-phenylthiopyridine nitroxide (39574-22-6)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 130 ℃; for 0.333333h; Microwave irradiation;

DOI:10.1016/j.mcat.2021.111981

Reference yield: 33.0%

pyridine N-oxide (694-59-7) + diphenyldisulfane (882-33-7) → 2-phenylthiopyridine nitroxide (39574-22-6)

Guidance literature:

With copper diacetate; potassium hydroxide; In toluene; at 140 ℃; for 48h; Schlenk technique;

upstream raw materials:

2-chloropyridine-N-oxide

thiophenolate

2-bromopyridine-N-oxide

thiophenol

Downstream raw materials:

2-benzenesulfonyl-pyridine N-oxide

2-phenylsulfanylpyridine