((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide

Base Information

Chemical Name:((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide
CAS No.:1387444-64-5
Molecular Formula:Br*C₃₆H₃₂O₆P
Molecular Weight:671.524
Hs Code.:

Synonyms:((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide

Chemical Property:

Purity/Quality:

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Technology Process of ((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide

There total 1 articles about ((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1387444-63-4
diethyl 2-(bromomethyl)-6-methylbenzofuro[5,6-b]furan-3,7-dicarboxylate

: 603-35-0
triphenylphosphine

: 1387444-64-5
((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide

Guidance literature:: In toluene; for 2.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2012.05.087

Reference yield:

: 1387444-64-5
((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide

: 104-88-1
4-chlorobenzaldehyde

: diethyl 2-(4-chlorostyryl)-6-methylbenzofuro[5,6-b]furan-3,7-dicarboxylate

Guidance literature:: ((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide; With lithium hydroxide monohydrate; In isopropyl alcohol; at 20 ℃; for 0.166667h; Inert atmosphere;

4-chlorobenzaldehyde; In isopropyl alcohol; for 2.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2012.05.087

Reference yield:

: 1387444-64-5
((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide

: 555-16-8
4-nitrobenzaldehdye

: diethyl 2-methyl-6-(4-nitrostyryl)benzofuro[5,6-b]furan-3,7-dicarboxylate

Guidance literature:: ((3,7-bis(ethoxycarbonyl)-6-methylbenzofuro[5,6-b]furan-2-yl)methyl)triphenylphosphonium bromide; With lithium hydroxide monohydrate; In isopropyl alcohol; at 20 ℃; for 0.166667h; Inert atmosphere;

4-nitrobenzaldehdye; In isopropyl alcohol; for 2.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2012.05.087