copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate

Base Information

• Chemical Name: copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate
• CAS No.: 216496-51-4
• Molecular Formula: C₃₇H₄₀BCuN₆O
• Molecular Weight: 659.121

Synonyms:copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate

Chemical Property of copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate

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Technology Process of copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate

There total 6 articles about copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(hydrotris(3-mesitylpyrazolyl)borate)Cu(thf) + carbon monoxide (201230-82-2) → copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate (216496-51-4)

Guidance literature:

In toluene; pentane; filtration; elem. anal.;

DOI:10.1021/ja982172q

Reference yield: 35.0%

(hydrotris(3-mesitylpyrazolyl)borate)Cu(thf) + N,N-diethyl-2-diazoacetamide (6112-00-1) → copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate (216496-51-4) + C41H51BCuN7

Guidance literature:

In toluene; at 70 ℃; for 1h; Temperature; Time; Overall yield = 0.35 g; Inert atmosphere;

DOI:10.1021/jacs.1c01483

Reference yield:

Na(1+)*HB(C3H2N2(C6H2(CH3)3))3(1-)=NaHB(C3H2N2(C6H2(CH3)3))3 → copper(I) carbon monoxide hydrotris(3-mesithylpyrazolil)borate (216496-51-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: pentane; toluene

In tetrahydrofuran; toluene; pentane;

DOI:10.1021/ja982172q

upstream raw materials:

carbon monoxide

N,N-diethyl-2-diazoacetamide

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