diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate

Base Information

• Chemical Name: diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate
• CAS No.: 1070910-51-8
• Molecular Formula: C₂₅H₂₆BrO₅P
• Molecular Weight: 517.356
• Mol file: 1070910-51-8.mol

Synonyms:diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate

Chemical Property of diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate

There total 1 articles about diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate (1070910-60-9) → diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate (1070910-51-8)

Guidance literature:

With tetrabutylammomium bromide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tetlet.2008.07.059

Reference yield: 88.0%

diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate (1070910-51-8) + 12-formyl-5,10,15,20-tetraphenyl-21H,23H-porphine → 2-(4'-(5,5'-dimethyl-[1,3]dioxane-2-yl)phenyl)ethynyl-5,10,15,20-tetraphenylporphyrin

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2008.07.059

upstream raw materials:

diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate