diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate

Base Information

• Chemical Name: diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate
• CAS No.: 1070910-60-9
• Molecular Formula: C₂₅H₂₇O₆P
• Molecular Weight: 454.46
• Mol file: 1070910-60-9.mol

Synonyms:diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate

Chemical Property of diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate

There total 1 articles about diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

diphenyl hydrogen phosphite (4712-55-4) + 4-(5,5-dimethyl-1,3-dioxan-2-yl)benzaldehyde (106456-88-6) → diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate (1070910-60-9)

Guidance literature:

With magnesium oxide; at 20 ℃;

DOI:10.1016/j.tetlet.2008.07.059

Reference yield: 64.0%

diphenyl hydroxy(4-(5,5-dimethyl-[1,3]-dioxane-2-yl)phenyl)methylphosphonate (1070910-60-9) → diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate (1070910-51-8)

Guidance literature:

With tetrabutylammomium bromide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tetlet.2008.07.059

upstream raw materials:

diphenyl hydrogen phosphite

4-(5,5-dimethyl-1,3-dioxan-2-yl)benzaldehyde

Downstream raw materials:

diphenyl bromo(4-(5,5-dimethyl-[1,3]dioxane-2-yl)phenyl)methylphosphonate