butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

Base Information

Chemical Name:butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate
CAS No.:1427195-96-7
Molecular Formula:C₁₉H₂₁N₅O₅S
Molecular Weight:431.472
Hs Code.:

Synonyms:butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

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Chemical Property of butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

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Technology Process of butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

There total 5 articles about butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 41891-17-2
N-butylcarbamoyl chloride

: 1427195-86-5
3-[(1Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(phenyl)methyl]-4-methyl-4,5-dihydro-1,2,4-oxadiazol-5-one

: 1427195-96-7
butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

Guidance literature:: With pyridine;

Reference yield:

: 1427201-45-3
(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(phenyl)acetonitrile

: 1427195-96-7
butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; potassium carbonate / isopropyl alcohol; water / 6 h / 80 °C

2: N,N-dimethyl-formamide / 6.5 h / 20 - 80 °C

3: potassium carbonate / acetonitrile; N,N-dimethyl-formamide / 20 °C

4: pyridine

With pyridine; hydroxylamine hydrochloride; potassium carbonate; In water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 1427201-29-3
(1Z,2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

: 1427195-96-7
butyl {4-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 6.5 h / 20 - 80 °C

2: potassium carbonate / acetonitrile; N,N-dimethyl-formamide / 20 °C

3: pyridine

With pyridine; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;