methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate

Base Information

Chemical Name:methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate
CAS No.:93394-80-0
Molecular Formula:C₃₆H₅₀N₄O₁₀S₂
Molecular Weight:762.946
Hs Code.:

methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate

Synonyms:methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate

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Chemical Property of methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate

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Technology Process of methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate

There total 8 articles about methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1069-29-0
L-cystine dimethyl ester

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 93394-80-0
methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate

Guidance literature:: With 2,3,5-trimethyl-pyridine; HATU; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/hlca.200890217

Reference yield: 90.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 32854-09-4
L-cystine dimethyl ester dihydrochloride

: 93394-80-0
methyl (6S,9R,14R)-6-benzyl-14-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)-9-(methoxycarbonyl)-2,2-dimethyl-4,7-dioxo-3-oxa-11,12-dithia-5,8-diazapentadecan-15-oate

Guidance literature:: L-cystine dimethyl ester dihydrochloride; With 4-methyl-morpholine; In dichloromethane; for 0.0833333h;

N-tert-butoxycarbonyl-L-phenylalanine; With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jacs.7b10227