C₂₅H₃₂O₄

Base Information

Chemical Name:C₂₅H₃₂O₄
CAS No.:1369677-40-6
Molecular Formula:C₂₅H₃₂O₄
Molecular Weight:396.527
Hs Code.:

C<sub>25</sub>H<sub>32</sub>O<sub>4</sub>

Synonyms:C₂₅H₃₂O₄

Suppliers and Price of C₂₅H₃₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₂O₄

Chemical Property:

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Technology Process of C₂₅H₃₂O₄

There total 9 articles about C₂₅H₃₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1369677-38-2
C₂₃H₃₀O₃

: 108-24-7
acetic anhydride

: 1369677-40-6
C₂₅H₃₂O₄

Guidance literature:: With dmap; triethylamine;
DOI:10.1016/j.tetlet.2012.02.049

Reference yield:

: 133604-03-2
ethyl (4S)-5-(((tert-butyldiphenyl)silyl)oxy)-4-methyl-2(E)-pentenoate

: 1369677-40-6
C₂₅H₃₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1: diisobutylaluminium hydride / diethyl ether

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate

3: copper(l) iodide

4: sodium hydride / tetrahydrofuran

5: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran

6: tetrabutyl ammonium fluoride / tetrahydrofuran

7: oxalyl dichloride; dimethyl sulfoxide; triethylamine

8: benzene

9: borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran

10: dmap; triethylamine

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; copper(l) iodide; borane-THF; oxalyl dichloride; diethyl (2S,3S)-tartrate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; diethyl ether; benzene; 9: Corey-Bakshi-Shibata reduction;
DOI:10.1016/j.tetlet.2012.02.049

Reference yield:

: 127665-68-3
(4S)-5-(tert-butyldiphenylsilyloxy)-4-methyl-2-penten-1-ol

: 1369677-40-6
C₂₅H₃₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate

2: copper(l) iodide

3: sodium hydride / tetrahydrofuran

4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran

5: tetrabutyl ammonium fluoride / tetrahydrofuran

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine

7: benzene

8: borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran

9: dmap; triethylamine

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; copper(l) iodide; borane-THF; oxalyl dichloride; diethyl (2S,3S)-tartrate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; dimethyl sulfoxide; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; benzene; 8: Corey-Bakshi-Shibata reduction;
DOI:10.1016/j.tetlet.2012.02.049