3-azidobenzyl iodide

Base Information

Chemical Name:3-azidobenzyl iodide
CAS No.:443299-18-1
Molecular Formula:C₇H₆IN₃
Molecular Weight:259.049
Hs Code.:

Synonyms:3-azidobenzyl iodide

Suppliers and Price of 3-azidobenzyl iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-azidobenzyl iodide

Chemical Property:

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Technology Process of 3-azidobenzyl iodide

There total 3 articles about 3-azidobenzyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 120692-80-0
3-azidobenzyl chloride

: 443299-18-1
3-azidobenzyl iodide

Guidance literature:: With sodium iodide; In acetone; at 20 ℃; for 12h;
DOI:10.1016/j.tet.2006.04.056

Reference yield:

: 89937-85-9
1-azido-3-hydroxymethylbenzene

: 443299-18-1
3-azidobenzyl iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / SOCl₂ / CH₂Cl₂ / 3 h / 0 °C

2: 91 percent / NaI / acetone / 12 h / 25 °C

With thionyl chloride; sodium iodide; In dichloromethane; acetone;
DOI:10.1016/j.tetlet.2007.03.087

Reference yield:

: 1877-77-6
3-aminobenzenemethanol

: 443299-18-1
3-azidobenzyl iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; sulfuric acid / H₂O / 0.5 h / cooling

1.2: 82 percent / sodium azide / H₂O / 16 h / 20 °C

2.1: 86 percent / thionyl chloride / CH₂Cl₂ / 3 h / 0 °C

3.1: 91 percent / sodium iodide / acetone / 12 h / 20 °C

With thionyl chloride; sulfuric acid; sodium iodide; sodium nitrite; In dichloromethane; water; acetone;
DOI:10.1016/j.tet.2006.04.056