3-azidobenzyl chloride

Base Information

Chemical Name:3-azidobenzyl chloride
CAS No.:120692-80-0
Molecular Formula:C₇H₆ClN₃
Molecular Weight:167.598
Hs Code.:

Synonyms:3-azidobenzyl chloride

Suppliers and Price of 3-azidobenzyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-azidobenzyl chloride

Chemical Property:

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Technology Process of 3-azidobenzyl chloride

There total 2 articles about 3-azidobenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 89937-85-9
1-azido-3-hydroxymethylbenzene

: 120692-80-0
3-azidobenzyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4039(98)01707-9

Reference yield:

: 1877-77-6
3-aminobenzenemethanol

: 120692-80-0
3-azidobenzyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; sulfuric acid / H₂O / 0.5 h / cooling

1.2: 82 percent / sodium azide / H₂O / 16 h / 20 °C

2.1: 86 percent / thionyl chloride / CH₂Cl₂ / 3 h / 0 °C

With thionyl chloride; sulfuric acid; sodium nitrite; In dichloromethane; water;
DOI:10.1016/j.tet.2006.04.056