trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

Base Information

Chemical Name:trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane
CAS No.:1097630-16-4
Molecular Formula:C₁₂H₁₇Br₂F₃S
Molecular Weight:410.136
Hs Code.:

Synonyms:trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

Suppliers and Price of trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 20 raw suppliers

Chemical Property of trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

There total 3 articles about trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 558-13-4
carbon tetrabromide

: 1097630-14-2
trans-4-(3,3,3-trifluoropropylthiomethyl)cyclohexanecarbaldehyde

: 1097630-16-4
trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

Guidance literature:: carbon tetrabromide; With triphenylphosphine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

trans-4-(3,3,3-trifluoropropylthiomethyl)cyclohexanecarbaldehyde; In dichloromethane; at 0 - 20 ℃; for 6.5h; Inert atmosphere;

Reference yield:

: 109004-13-9
[4-(p-toluenesulfonyloxymethyl)cyclohexyl]methanol

: 1097630-16-4
trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium thioacetate / dimethyl sulfoxide / 7 h / 20 - 60 °C

1.2: 1 h / 0 °C

1.3: 6 h / 60 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3.5 h / -78 - -50 °C / Inert atmosphere

2.2: 19.5 h / -50 - 20 °C / Inert atmosphere

3.1: triphenylphosphine / dichloromethane / 2 h / 0 °C / Inert atmosphere

3.2: 6.5 h / 0 - 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; triphenylphosphine; potassium thioacetate; In dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1233934-87-6
4-(3,3,3-trifluoropropylthiomethyl)cyclohexanemethanol

: 1097630-16-4
trans-1-(2,2-dibromovinyl)-4-(3,3,3-trifluoropropylthiomethyl)cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3.5 h / -78 - -50 °C / Inert atmosphere

1.2: 19.5 h / -50 - 20 °C / Inert atmosphere

2.1: triphenylphosphine / dichloromethane / 2 h / 0 °C / Inert atmosphere

2.2: 6.5 h / 0 - 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; triphenylphosphine; In dichloromethane;