C₄₀H₅₃NO₇S₆

Base Information

Chemical Name:C₄₀H₅₃NO₇S₆
CAS No.:1443384-36-8
Molecular Formula:C₄₀H₅₃NO₇S₆
Molecular Weight:852.259
Hs Code.:

C<sub>40</sub>H<sub>53</sub>NO<sub>7</sub>S<sub>6</sub>

Synonyms:C₄₀H₅₃NO₇S₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₀H₅₃NO₇S₆

Chemical Property:

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Technology Process of C₄₀H₅₃NO₇S₆

There total 5 articles about C₄₀H₅₃NO₇S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 846571-61-7
N-tosyl-2-[4-(ethylthio)-5-(2-cyanoethylthio)-(1,3)-dithiole-2-ylidene]-(1,3)-dithiolo[4,5-c]pyrrole

: 1443384-35-7
C₃₀H₄₅IO₇

: 1443384-36-8
C₄₀H₅₃NO₇S₆

Guidance literature:: N-tosyl-2-[4-(ethylthio)-5-(2-cyanoethylthio)-(1,3)-dithiole-2-ylidene]-(1,3)-dithiolo[4,5-c]pyrrole; C₃₀H₄₅IO₇; With cesiumhydroxide monohydrate; In tetrahydrofuran; methanol; at 20 ℃; for 26h; Inert atmosphere;

With sodium methylate; In tetrahydrofuran; methanol; for 0.5h; Inert atmosphere; Reflux;
DOI:10.1039/c3cc42201a

Reference yield:

: 224298-61-7
1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

: 1443384-36-8
C₄₀H₅₃NO₇S₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium iodide / acetone / 27 h / Inert atmosphere; Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / Inert atmosphere; Reflux

3.1: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

4.1: sodium iodide / acetone / 19 h / Inert atmosphere; Reflux

5.1: cesiumhydroxide monohydrate / tetrahydrofuran; methanol / 26 h / 20 °C / Inert atmosphere

5.2: 0.5 h / Inert atmosphere; Reflux

With cesiumhydroxide monohydrate; potassium carbonate; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c3cc42201a

Reference yield:

: 1443384-32-4
C₁₈H₂₉IO₇

: 1443384-36-8
C₄₀H₅₃NO₇S₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / Inert atmosphere; Reflux

2.1: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

3.1: sodium iodide / acetone / 19 h / Inert atmosphere; Reflux

4.1: cesiumhydroxide monohydrate / tetrahydrofuran; methanol / 26 h / 20 °C / Inert atmosphere

4.2: 0.5 h / Inert atmosphere; Reflux

With cesiumhydroxide monohydrate; potassium carbonate; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c3cc42201a