2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide

Base Information

Chemical Name:2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide
CAS No.:153524-89-1
Molecular Formula:C₁₈H₁₇NO₅S
Molecular Weight:359.403
Hs Code.:

Synonyms:2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide

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Chemical Property of 2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide

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Technology Process of 2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide

There total 3 articles about 2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 153524-93-7
(E)-1-(Phenylsulfonyl)-3-(α-methyl-β-methoxyvinyl)indole

: 153524-89-1
2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide

Guidance literature:: With tetraphenylporphyrine; oxygen; In dichloromethane; at -78 ℃; for 0.333333h; Irradiation;
DOI:10.1021/jo00079a032

Reference yield:

: 99532-45-3
3-acetyl-1-benzenesulfonylindole

: 153524-89-1
2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.1 M n-BuLi / tetrahydrofuran; hexane / 1.) -30 deg C, 1.0 h, 2.) -78 deg C, 2 h; r.t., 30 min

2: 80 percent / tetraphenylporphyrine, O₂ / CH₂Cl₂ / 0.33 h / -78 °C / Irradiation

With n-butyllithium; tetraphenylporphyrine; oxygen; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/jo00079a032

Reference yield:

: 117760-49-3
3-(1-methylethenyl)-1-phenylsulfonyl-1H-indole

: 153524-89-1
2-(1-Benzenesulfonyl-1H-indol-3-yl)-1-methoxy-prop-2-en-1-yl-hydroperoxide

Guidance literature:: Multi-step reaction with 3 steps

1: 15 percent Spectr_. / methylene blue, O₂ / acetone-d6 / 1 h / -78 °C / Irradiation

2: 2.1 M n-BuLi / tetrahydrofuran; hexane / 1.) -30 deg C, 1.0 h, 2.) -78 deg C, 2 h; r.t., 30 min

3: 80 percent / tetraphenylporphyrine, O₂ / CH₂Cl₂ / 0.33 h / -78 °C / Irradiation

With n-butyllithium; tetraphenylporphyrine; oxygen; methylene blue; In tetrahydrofuran; hexane; dichloromethane; acetone;
DOI:10.1021/jo00079a032