ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

Base Information

Chemical Name:ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate
CAS No.:86459-06-5
Molecular Formula:C₄₂H₇₂N₄O₇
Molecular Weight:745.056
Hs Code.:

Synonyms:ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

Suppliers and Price of ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

There total 6 articles about ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 86459-05-4
17-benzyloxycarbonylamino-10-oxo-9-azaheptadecanoic acid

: 86459-04-3
17-amino-10-oxo-9-azaoctadecanoic acid ethyl ester hydrochloride

: 86459-06-5
ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

Guidance literature:: With triethylamine; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide; at -18 - 25 ℃;
DOI:10.1248/cpb.31.737

Reference yield:

: 1074-51-7
cyclooctanone oxime

: 86459-06-5
ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

Guidance literature:: Multi-step reaction with 4 steps

2: 89 percent / Et₃N, DMAP, DCC / CH₂Cl₂ / 24 h / 0 - 20 °C

3: 84 percent / 0.5N NaOH / acetone; H₂O / 24 h / Ambient temperature

4: 84 percent / Et₃N, isobutyl chlorocarbonate / dimethylformamide; tetrahydrofuran / -18 - 25 °C

With dmap; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; isobutyl chloroformate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1248/cpb.31.737

Reference yield:

: 23434-40-4
8-(benzyloxycarbonylamino)octanoic acid

: 86459-06-5
ethyl 35-benzyloxycarbonylamino-10,19,28-trioxo-9,18,27-triazapentatriacontanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / Et₃N, DMAP, DCC / CH₂Cl₂ / 24 h / 0 - 20 °C

2: 84 percent / 0.5N NaOH / acetone; H₂O / 24 h / Ambient temperature

3: 84 percent / Et₃N, isobutyl chlorocarbonate / dimethylformamide; tetrahydrofuran / -18 - 25 °C

With dmap; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; isobutyl chloroformate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1248/cpb.31.737