Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide

Base Information

Chemical Name:Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide
CAS No.:128797-64-8
Molecular Formula:C₁₆H₁₈N₂O₃S
Molecular Weight:318.397
Hs Code.:

Synonyms:Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide

Suppliers and Price of Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide

Chemical Property:

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Technology Process of Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide

There total 2 articles about Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 128797-62-6
2,6-dioxo-4,4-dimethylcyclohexylthiocarbohydrazide

: 98-88-4
benzoyl chloride

: 128797-64-8
Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide

Guidance literature:: With triethylamine; In chloroform; 1 h at 5 deg C, then 4 h at room temp.;

Reference yield:

: 111604-11-6
2-(5,5-dimethyl-1,3-dioxocyclohexane-2-ylidene)-1,3-dithietane

: 128797-64-8
Benzoic acid N'-(4,4-dimethyl-2,6-dioxo-cyclohexanecarbothioyl)-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / hydrazine monohydrate / acetonitrile / 2.5 h / 10 - 15 °C

2: 76 percent / triethylamine / CHCl₃ / 1 h at 5 deg C, then 4 h at room temp.

With hydrazine hydrate; triethylamine; In chloroform; acetonitrile;