3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol

Base Information

Chemical Name:3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol
CAS No.:1620831-73-3
Molecular Formula:C₃₀H₂₄O₄S
Molecular Weight:480.584
Hs Code.:

Synonyms:3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol

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Chemical Property of 3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol

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Technology Process of 3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol

There total 3 articles about 3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1620831-72-2
1-phenyl-2-[2-(2-phenylethynyl)phenoxy]-4-(phenylsulfonyl)butan-1-one

: 1620831-73-3
3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol

Guidance literature:: With iron(III) chloride; potassium acetate; In acetonitrile; at 120 ℃; for 24h; Molecular sieve;
DOI:10.1055/s-0033-1338557

Reference yield:

: 599-94-0
1,2-bis(phenylsulfonyl)ethane

: 1620831-73-3
3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / toluene / 36 h / 120 °C

2: dichloro bis(acetonitrile) palladium(II); copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C

3: iron(III) chloride; potassium acetate / acetonitrile / 24 h / 120 °C / Molecular sieve

With iron(III) chloride; dichloro bis(acetonitrile) palladium(II); copper(l) iodide; potassium tert-butylate; potassium acetate; triethylamine; In tetrahydrofuran; toluene; acetonitrile; 2: |Sonogashira Cross-Coupling;
DOI:10.1055/s-0033-1338557

Reference yield:

: 1620831-61-9
2-(2-iodophenoxy)-1-phenyl-4-(phenylsulfonyl)butan-1-one

: 1620831-73-3
3-(2-hydroxyphenyl)-4-phenyl-2-[2-(phenylsulfonyl)ethyl]naphthalen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro bis(acetonitrile) palladium(II); copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C

2: iron(III) chloride; potassium acetate / acetonitrile / 24 h / 120 °C / Molecular sieve

With iron(III) chloride; dichloro bis(acetonitrile) palladium(II); copper(l) iodide; potassium acetate; triethylamine; In tetrahydrofuran; acetonitrile; 1: |Sonogashira Cross-Coupling;
DOI:10.1055/s-0033-1338557