4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate

Base Information

Chemical Name:4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate
CAS No.:1394236-27-1
Molecular Formula:C₃₀H₃₂ClN₃O₉
Molecular Weight:614.052
Hs Code.:

Synonyms:4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate

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Chemical Property of 4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate

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Technology Process of 4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate

There total 2 articles about 4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1394236-21-5
C₂₃H₂₇ClO₉

: 55116-31-9
1-(azidomethyl)-4-hydroxybenzene

: 1394236-27-1
4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere; Cooling with ice;
DOI:10.1039/c2jm33612j

Reference yield:

: 623-05-2
(4-hydroxyphenyl)methanol

: 1394236-27-1
4-(azidomethyl)phenyl 4-(3-chloro-4-(2,5,8,11-tetraoxatridecan-13-yloxy)benzoyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; tetrachloromethane; triphenylphosphine / N,N-dimethyl-formamide

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 16 h / 20 °C / Inert atmosphere; Cooling with ice

With tetrachloromethane; dmap; sodium azide; dicyclohexyl-carbodiimide; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2jm33612j