cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide

Base Information

Chemical Name:cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide
CAS No.:1350980-66-3
Molecular Formula:C₃₆H₃₈N₂O₉
Molecular Weight:642.706
Hs Code.:

Synonyms:cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide

Chemical Property:

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Technology Process of cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide

There total 7 articles about cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate: 1308813-97-9
4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

: 1161014-56-7
2-amino-N-cyclopentyl-3-phenyl-propionamide

: 1350980-66-3
cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.10.024

Reference yield:

: 1026875-42-2
C₁₉H₂₈N₂O₃

: 1350980-66-3
cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane

2: dmap; triethylamine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

With dmap; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2011.10.024

Reference yield:

: 3590-93-0,85440-15-9,123287-54-7,123287-57-0
4'-demethyl-4-deoxypodophyllotoxin

: 1350980-66-3
cyclopentyl N-(1-oxyl-4'-demethyl-4-deoxypodophyllic)-L-phenylalanine amide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2011.10.024