4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

Base Information

Chemical Name:4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate
CAS No.:1308813-97-9
Molecular Formula:C₂₈H₂₃NO₁₁
Molecular Weight:549.491
Hs Code.:

Synonyms:4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

Suppliers and Price of 4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

Chemical Property:

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Technology Process of 4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

There total 4 articles about 4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3590-93-0,85440-15-9,123287-54-7,123287-57-0
4'-demethyl-4-deoxypodophyllotoxin

: 7693-46-1
4-Nitrophenyl chloroformate

4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate: 1308813-97-9
4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

Guidance literature:: 4-Nitrophenyl chloroformate; With pyridine; In dichloromethane; Inert atmosphere;

4'-demethyl-4-deoxypodophyllotoxin; In dichloromethane; at 20 ℃; for 0.75h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.06.004

Reference yield:

: 518-28-5
podofilox

4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate: 1308813-97-9
4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen bromide / dichloromethane

2.1: palladium 10% on activated carbon; hydrogen; acetic acid / 5 h / 95 °C / 1520.1 Torr

3.1: pyridine / dichloromethane / Inert atmosphere

3.2: 0.75 h / 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen bromide; hydrogen; acetic acid; In dichloromethane;
DOI:10.1016/j.ejmech.2011.06.004

Reference yield:

: 477-51-0,6258-33-9,17187-81-4,17301-90-5,19186-35-7,24150-39-8,31892-96-3,55568-81-5,64550-41-0,69222-20-4,75171-57-2,83023-41-0,100348-38-7
deoxypodophyllotoxin

4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate: 1308813-97-9
4'-demethyl-4-deoxypodophyllotoxin 4'-(p-nitrophenyl) carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanesulfonic acid; sodium iodide

2.1: pyridine / dichloromethane / Inert atmosphere

2.2: 0.75 h / 20 °C / Inert atmosphere

With pyridine; methanesulfonic acid; sodium iodide; In dichloromethane;
DOI:10.1016/j.ejmech.2011.06.004