[(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester

Base Information

Chemical Name:[(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester
CAS No.:656827-45-1
Molecular Formula:C₁₀H₁₀F₃NO₂S₃
Molecular Weight:329.388
Hs Code.:

Synonyms:[(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester

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Chemical Property of [(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester

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Technology Process of [(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester

There total 1 articles about [(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-dimercaptomethylene-4-trifluoromethyl-benzenesulfonamide

: 74-88-4
methyl iodide

: 656827-45-1
[(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester

Guidance literature:: In N,N-dimethyl-formamide; for 2h;
DOI:10.1021/jm031019q

Reference yield: 89.0%

: 59074-26-9
3-(4-chlorophenyl)-4-phenyl-4,5-dihydro-1H-pyrazole

: 656827-45-1
[(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester

: 656827-49-5
3-(4-chlorophenyl)-N-{[4-(trifluoromethyl)phenyl]sulfonyl}-4-phenyl-4,5-dihydro-1H-pyrazole-1-carboximidothioic acid methyl ester

Guidance literature:: With triethylamine; In acetonitrile; for 36h; Heating;
DOI:10.1021/jm031019q

Reference yield:

: 656827-45-1
[(4-(trifluoromethyl)phenyl)sulfonyl]dithioimidocarbonic acid dimethyl ester

: (-)-3-(4-chlorophenyl)-N'-methyl-N-{[(4-trifluoromethyl)phenyl]sulfonyl}-4-phenyl-4,5-dihydro-1H-pyrazole-1-carboxamidine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / Et₃N / acetonitrile / 36 h / Heating

2: 76 percent / methanol; H₂O; CH₂Cl₂ / 6 h / 20 °C

3: heptane; propan-2-ol / chiral preparative HPLC

With triethylamine; In methanol; n-heptane; dichloromethane; water; isopropyl alcohol; acetonitrile;
DOI:10.1021/jm031019q