2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide

Base Information

Chemical Name:2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide
CAS No.:117566-76-4
Molecular Formula:C₁₄H₁₉N₂O₃
Molecular Weight:263.316
Hs Code.:

Synonyms:2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide

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Technology Process of 2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide

There total 11 articles about 2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 41359-25-5
1,3-dihydroxyl-2-(4'-methoxyphen-1'-yl)-4,4,5,5-tetramethylimidazolidine

: 117566-76-4
2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide

Guidance literature:: With lead dioxide; In methanol; at 20 ℃; for 0.333333h;
DOI:10.1016/j.bmc.2007.02.023

Reference yield: 73.0%

: 696-62-8
para-iodoanisole

: NN-Au₁,3-dimesitylimidazolidin-2-ylidene

: 117566-76-4
2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 66 ℃; for 3h; Reagent/catalyst; Inert atmosphere;
DOI:10.1246/bcsj.20180033

Reference yield: 73.0%

: 696-62-8
para-iodoanisole

: NN-Cu(2,9-bis(2,6-dimethoxyphenyl)-1,10-phenanthroline)

: 117566-76-4
2-methoxyphenyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxy 3-oxide

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene; In tetrahydrofuran; at 66 ℃; for 0.25h; Inert atmosphere;
DOI:10.1246/bcsj.20180033