C₂₈H₃₄O₆

Base Information

Chemical Name:C₂₈H₃₄O₆
CAS No.:827325-46-2
Molecular Formula:C₂₈H₃₄O₆
Molecular Weight:466.574
Hs Code.:

C<sub>28</sub>H<sub>34</sub>O<sub>6</sub>

Synonyms:C₂₈H₃₄O₆

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Chemical Property of C₂₈H₃₄O₆

Chemical Property:

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Technology Process of C₂₈H₃₄O₆

There total 11 articles about C₂₈H₃₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 827325-42-8
C₂₈H₃₄O₅

: 827325-46-2
C₂₈H₃₄O₆

Guidance literature:: With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; In decane; benzene; at 20 ℃; for 10h;
DOI:10.1021/ja044123l

Reference yield:

: 454482-62-3
1-(((2-(chloromethyl)allyl)oxy)methyl)-4-methoxybenzene

: 827325-46-2
C₂₈H₃₄O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: 98 percent / KH / tetrahydrofuran / Heating

2.1: 76 percent / Hoveyda-Grubbs catalyst / toluene / 30 h / Heating

3.1: aq. HCl / tetrahydrofuran / 3 h / Heating

4.1: 1.9 g / NaBH₄ / ethanol; tetrahydrofuran / 0.25 h / 0 °C

5.1: PPh₃; imidazole; I₂ / tetrahydrofuran / 3 h / 0 °C

5.2: 94 percent / t-BuOK / tetrahydrofuran; dimethylsulfoxide / 20 °C

6.1: 49 percent / SeO₂; aq. AcOH; t-BuOOH / CH₂Cl₂; decane / 2 h / 20 °C

7.1: 74 percent / Dess-Martin periodinane / CH₂Cl₂ / 1.5 h / -40 - 10 °C

8.1: 74 percent / aq. RhCl₃ / aq. ethanol / 0.58 h / 115 °C

9.1: 94 percent / P(OMe)3; O₂; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.75 h / -40 °C

10.1: 73 percent / VO(acac)2; t-BuOOH / benzene; decane / 10 h / 20 °C

With 1H-imidazole; hydrogenchloride; tert.-butylhydroperoxide; [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; sodium tetrahydroborate; rhodium(III) chloride; selenium(IV) oxide; bis(acetylacetonate)oxovanadium; potassium tert-butylate; iodine; oxygen; potassium hydride; Dess-Martin periodane; acetic acid; triphenylphosphine; phosphorous acid trimethyl ester; In tetrahydrofuran; decane; ethanol; dichloromethane; toluene; tert-butyl alcohol; benzene; 2.1: Grubbs reaction;
DOI:10.1021/ja044123l

Reference yield:

: C₂₀H₃₀O₃

: 827325-46-2
C₂₈H₃₄O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: 98 percent / KH / tetrahydrofuran / Heating

2.1: 76 percent / Hoveyda-Grubbs catalyst / toluene / 30 h / Heating

3.1: aq. HCl / tetrahydrofuran / 3 h / Heating

4.1: 1.9 g / NaBH₄ / ethanol; tetrahydrofuran / 0.25 h / 0 °C

5.1: PPh₃; imidazole; I₂ / tetrahydrofuran / 3 h / 0 °C

5.2: 94 percent / t-BuOK / tetrahydrofuran; dimethylsulfoxide / 20 °C

6.1: 49 percent / SeO₂; aq. AcOH; t-BuOOH / CH₂Cl₂; decane / 2 h / 20 °C

7.1: 74 percent / Dess-Martin periodinane / CH₂Cl₂ / 1.5 h / -40 - 10 °C

8.1: 74 percent / aq. RhCl₃ / aq. ethanol / 0.58 h / 115 °C

9.1: 94 percent / P(OMe)3; O₂; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.75 h / -40 °C

10.1: 73 percent / VO(acac)2; t-BuOOH / benzene; decane / 10 h / 20 °C

With 1H-imidazole; hydrogenchloride; tert.-butylhydroperoxide; [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; sodium tetrahydroborate; rhodium(III) chloride; selenium(IV) oxide; bis(acetylacetonate)oxovanadium; potassium tert-butylate; iodine; oxygen; potassium hydride; Dess-Martin periodane; acetic acid; triphenylphosphine; phosphorous acid trimethyl ester; In tetrahydrofuran; decane; ethanol; dichloromethane; toluene; tert-butyl alcohol; benzene; 2.1: Grubbs reaction;
DOI:10.1021/ja044123l