2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide

Base Information

Chemical Name:2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide
CAS No.:1417885-99-4
Molecular Formula:C₁₇H₁₁F₃N₆O₂
Molecular Weight:388.309
Hs Code.:

Synonyms:2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide

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Chemical Property of 2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide

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Technology Process of 2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide

There total 3 articles about 2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1417885-98-3
2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoic acid

: 1417885-99-4
2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In isopropyl alcohol; at 20 ℃; Inert atmosphere;

Reference yield:

: 1417885-96-1
3-bromo-1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazole

: 1417885-99-4
2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 0.5 h / 140 °C / Microwave irradiation

2: sodium hydroxide / tetrahydrofuran; methanol

3: triethylamine; diphenyl phosphoryl azide / isopropyl alcohol / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; sodium hydrogencarbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; water; isopropyl alcohol;

Reference yield:

: 103962-05-6
1-iodo-4-(trifluoromethoxy)benzene

: 1417885-99-4
2-methyl-4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)benzoyl azide

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; caesium carbonate / dimethyl sulfoxide / 20 h / 100 °C / Inert atmosphere

2: sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 0.5 h / 140 °C / Microwave irradiation

3: sodium hydroxide / tetrahydrofuran; methanol

4: triethylamine; diphenyl phosphoryl azide / isopropyl alcohol / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; sodium hydrogencarbonate; caesium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; water; dimethyl sulfoxide; isopropyl alcohol;