allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

Base Information

Chemical Name:allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine
CAS No.:155177-93-8
Molecular Formula:C₄₀H₄₈N₄O₉Si
Molecular Weight:756.928
Hs Code.:

allyl N-(9-fluorenylmethoxycarbonyl)-<O-<2-azido-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-α-D-galactopyranosyl>-(1<*>3)>-L-serine

Synonyms:allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

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Chemical Property of allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

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Technology Process of allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

There total 9 articles about allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.8%

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 155177-91-6
2-azido-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-β-D-galactopyranosyl fluoride

: allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

: 155177-93-8
allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

Guidance literature:: With zirconocene dichloride; 4 A molecular sieve; silver perchlorate; In dichloromethane; at -20 - 25 ℃; for 10h;
DOI:10.1016/0008-6215(94)00362-J

Reference yield: 85.3%

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 155177-90-5
2-azido-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-α-D-galactopyranosyl fluoride

: allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

: 155177-93-8
allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

Guidance literature:: With zirconocene dichloride; 4 A molecular sieve; silver perchlorate; In dichloromethane; at -20 - 25 ℃; for 10h;
DOI:10.1016/0008-6215(94)00362-J

Reference yield:

: 155177-88-1
2-azido-4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-α-D-galactopyranosyl fluoride

: 155177-93-8
allyl N-(9-fluorenylmethoxycarbonyl)--(1<*>3)>-L-serine

Guidance literature:: Multi-step reaction with 3 steps

1: 99.9 percent / hydrazine acetate / toluene; ethanol / 0.5 h / Ambient temperature

2: 91.4 percent / imidazole, DMAP / dimethylformamide / Ambient temperature

3: 85.3 percent / AgClO₄, Cp₂ZrCl₂, 4A molecular sieves / CH₂Cl₂ / 10 h / -20 - 25 °C

With 1H-imidazole; dmap; zirconocene dichloride; 4 A molecular sieve; silver perchlorate; hydrazinium monoacetate; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0008-6215(94)00362-J