C₄₇H₃₁N₅NiO₃

Base Information

Chemical Name:C₄₇H₃₁N₅NiO₃
CAS No.:1259580-77-2
Molecular Formula:C₄₇H₃₁N₅NiO₃
Molecular Weight:772.485
Hs Code.:

C<sub>47</sub>H<sub>31</sub>N<sub>5</sub>NiO<sub>3</sub>

Synonyms:C₄₇H₃₁N₅NiO₃

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Chemical Property of C₄₇H₃₁N₅NiO₃

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Technology Process of C₄₇H₃₁N₅NiO₃

There total 5 articles about C₄₇H₃₁N₅NiO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1259580-75-0
C₄₇H₂₉N₅NiO₂

: 1259580-77-2
C₄₇H₃₁N₅NiO₃

Guidance literature:: C₄₇H₂₉N₅NiO₂; With isopropyl alcohol; potassium hydroxide; at 20 ℃; for 0.25h;

With water; citric acid; In isopropyl alcohol;
DOI:10.1021/ol102691s

Reference yield:

: 42565-85-5
(β-formyl-meso-tetraphenylporphyrinato)nickel(II)

: 1259580-77-2
C₄₇H₃₁N₅NiO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate

2.1: 5,15,10,20-tetraphenylporphyrin / 1,2-dichloro-benzene / 1.5 h / 20 °C / Irradiation

2.2: 0.5 h / Reflux

3.1: isopropyl alcohol; potassium hydroxide / 0.25 h / 20 °C

With 5,15,10,20-tetraphenylporphyrin; potassium carbonate; isopropyl alcohol; potassium hydroxide; In 1,2-dichloro-benzene;
DOI:10.1021/ol102691s

Reference yield:

: 202463-09-0
NiN₄C₂₀H₆(C₆H₅)4C₂H₂NCH₃

: 1259580-77-2
C₄₇H₃₁N₅NiO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: 5,15,10,20-tetraphenylporphyrin / 1,2-dichloro-benzene / 1.5 h / 20 °C / Irradiation

1.2: 0.5 h / Reflux

2.1: isopropyl alcohol; potassium hydroxide / 0.25 h / 20 °C

With 5,15,10,20-tetraphenylporphyrin; isopropyl alcohol; potassium hydroxide; In 1,2-dichloro-benzene;
DOI:10.1021/ol102691s