methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate

Base Information

Chemical Name:methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate
CAS No.:1454845-40-9
Molecular Formula:C₁₇H₂₄N₂O₆S
Molecular Weight:384.453
Hs Code.:

Synonyms:methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate

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Chemical Property of methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate

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Technology Process of methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate

There total 2 articles about methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2491-20-5
L-alanine methyl ester hydrochloride

: 212204-36-9
Cbz-Pro-ψ[CH2SO2]-Cl

: 1454845-40-9
methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate

Guidance literature:: With triethylamine; In dichloromethane; at 35 ℃; Cooling with ice;
DOI:10.1016/j.tet.2013.08.028

Reference yield:

: 101250-72-0
(S)-2-Acetylsulfanylmethyl-pyrrolidine-1-carboxylic acid benzyl ester

: 1454845-40-9
methyl (S)-N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]alaninate

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide; hydrogenchloride / water; acetonitrile / 10 - 20 °C

2: triethylamine / dichloromethane / 35 °C / Cooling with ice

With hydrogenchloride; N-chloro-succinimide; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2013.08.028