TH-1344

Base Information

Chemical Name:TH-1344
CAS No.:1196073-11-6
Molecular Formula:C₂₅H₂₆Cl₂N₄O₈S₂
Molecular Weight:645.541
Hs Code.:

Synonyms:TH-1344

Suppliers and Price of TH-1344

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TH-1344

Chemical Property:

Purity/Quality:

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Technology Process of TH-1344

There total 8 articles about TH-1344 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1196072-02-2
3-(4-(N,N-bis-(2-chloroethyl)amino)phenoxysulfonyl-(2-aminopyridin-5-yl-methyl))methyl-2-nitrothiophene

: 13831-31-7
Acetoxyacetyl chloride

: 1196073-11-6
TH-1344

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 6373-46-2
p-benzyloxyaniline

: 1196073-11-6
TH-1344

Guidance literature:: Multi-step reaction with 8 steps

1: acetic acid / water / -78 - 20 °C

2: trichlorophosphate / 1 h / 100 °C

3: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water; ethyl acetate / 3 h

4: triethylamine / dichloromethane / 0 - 20 °C

5: potassium tert-butylate / tetrahydrofuran; dichloromethane / 1 h / -50 °C

6: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h

7: trifluoroacetic acid / dichloromethane / 0 - 20 °C

8: triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; potassium tert-butylate; hydrogen; acetic acid; triethylamine; triphenylphosphine; trifluoroacetic acid; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; 6: Mitsunobu reaction;

Reference yield:

: 101582-69-8
4--O-benzylphenol

: 1196073-11-6
TH-1344

Guidance literature:: Multi-step reaction with 7 steps

1: trichlorophosphate / 1 h / 100 °C

2: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water; ethyl acetate / 3 h

3: triethylamine / dichloromethane / 0 - 20 °C

4: potassium tert-butylate / tetrahydrofuran; dichloromethane / 1 h / -50 °C

5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h

6: trifluoroacetic acid / dichloromethane / 0 - 20 °C

7: triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; potassium tert-butylate; hydrogen; triethylamine; triphenylphosphine; trifluoroacetic acid; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; 5: Mitsunobu reaction;