(Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

Base Information

Chemical Name:(Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran
CAS No.:1311273-28-5
Molecular Formula:C₂₈H₂₆O
Molecular Weight:378.514
Hs Code.:

Synonyms:(Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

Suppliers and Price of (Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

There total 4 articles about (Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 534-22-5
2-methylfuran

: 1311273-16-1
(E)-2-benzylidene-4-(cyclohexen-1-yl)-1-phenylbut-3-yn-1-ol

: 1311273-28-5
(Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo2004023

Reference yield:

: 33603-90-6
(2Z)-2-bromo-3-phenyl-2-propenal

: 1311273-28-5
(Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; boron trifluoride diethyl etherate; triethylamine; In tetrahydrofuran; hexane; dichloromethane; 3.1: Friedel Crafts alkylation;
DOI:10.1021/jo2004023

Reference yield:

: 931-49-7
1-ethenylcyclohexene

: 1311273-28-5
(Z)-2-(2-benzylidene-4-cyclohexen-1-yl-1-phenylbut-3-ynyl)-5-methylfuran

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; boron trifluoride diethyl etherate; triethylamine; In tetrahydrofuran; hexane; dichloromethane; 3.1: Friedel Crafts alkylation;
DOI:10.1021/jo2004023