2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

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Chemical Name:2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole
CAS No.:1357384-09-8
Molecular Formula:C₃₇H₃₃N₅O₅S
Molecular Weight:659.766
Hs Code.:

Synonyms:2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

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Chemical Property of 2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

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Technology Process of 2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

There total 4 articles about 2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1357384-08-7
2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

: 1357384-09-8
2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 7h;
DOI:10.1002/jhet.668

Reference yield:

: 108446-63-5
1-(1-biphenyl-4-yl-ethylidene)-2-phenylhydrazine

: 1357384-09-8
2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / 1.25 h / Cooling with ice

1.2: 2 h / 0 °C / Reflux

2.1: 5 h / Reflux

3.1: sodium acetate / ethanol / 5 h / Reflux

4.1: potassium hydroxide / water; acetone / 7 h / 20 °C

5.1: ammonia / methanol / 7 h / 20 °C

With ammonia; sodium acetate; potassium hydroxide; trichlorophosphate; In methanol; ethanol; water; acetone; 1.1: Vilsmeier-Haack reaction / 1.2: Vilsmeier-Haack reaction;
DOI:10.1002/jhet.668

Reference yield:

: 1357384-03-2
2-{[[3-(biphenyl-4-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-4-phenyl-2,3-dihydrothiazole

: 1357384-09-8
2-{[[3-(biphenyl-3-yl)-1-phenyl-1H-pyrazol-4-yl]methylene]-hydrazono}-3-(β-D-glucopyranosyl)-4-phenyl-2,3-dihydrothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / water; acetone / 7 h / 20 °C

2: ammonia / methanol / 7 h / 20 °C

With ammonia; potassium hydroxide; In methanol; water; acetone;
DOI:10.1002/jhet.668