(1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

Base Information

Chemical Name:(1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate
CAS No.:151910-10-0
Molecular Formula:C₁₆H₂₁NO₄
Molecular Weight:291.347
Hs Code.:

(1S,2R)-(E)-methyl 1-<N-<<(1,1-dimethylethyl)oxy>carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

Synonyms:(1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

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Chemical Property of (1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

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Technology Process of (1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

There total 10 articles about (1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 180322-87-6
1-(methoxycarbonyl)-2-phenylcyclopropanecarboxylic acid

: 151910-10-0
(1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, diphenylphosphoryl azide / 2-methyl-propan-2-ol; hexane / Heating

2: 2-methyl-propan-2-ol; hexane / Heating

With diphenylphosphoranyl azide; triethylamine; In hexane; tert-butyl alcohol;
DOI:10.1021/ja9604931

Reference yield:

: 180322-84-3
monomethyl (1S,2R)-2-phenylcyclopropane-1,1-dicarboxylate

: 151910-10-0
(1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / K₂CO₃

2: 73 percent / aq. NaOH / methanol

3: Et₃N, diphenylphosphoryl azide / 2-methyl-propan-2-ol; hexane / Heating

4: 2-methyl-propan-2-ol; hexane / Heating

With sodium hydroxide; diphenylphosphoranyl azide; potassium carbonate; triethylamine; In methanol; hexane; tert-butyl alcohol;
DOI:10.1021/ja9604931

Reference yield:

: 72397-56-9
(2R)-dimethyl 2-phenylcyclopropane-1,1-dicarboxylate

: 151910-10-0
(1S,2R)-(E)-methyl 1-carbonyl>amino>-2-phenylcyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / aq. NaOH / methanol

2: Et₃N, diphenylphosphoryl azide / 2-methyl-propan-2-ol; hexane / Heating

3: 2-methyl-propan-2-ol; hexane / Heating

With sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In methanol; hexane; tert-butyl alcohol;
DOI:10.1021/ja9604931