(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester

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Chemical Name:(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester
CAS No.:918304-56-0
Molecular Formula:C₄₁H₃₇BrINO₅
Molecular Weight:830.557
Hs Code.:

Synonyms:(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester

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Chemical Property of (Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester

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Technology Process of (Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester

There total 1 articles about (Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 918304-92-4
(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid

: 2040-86-0
2-bromo-6-iodophenol

: 918304-56-0
(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 14h;
DOI:10.1039/b609604b

Reference yield: 49.0%

: 918304-56-0
(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-bromo-6-iodo-phenyl ester

: 918304-57-1
(S)-3-[4-benzyloxy-3-(7-bromo-2-oxo-3-vinyl-2,3-dihydro-benzofuran-3-yl)-phenyl]-2-dibenzylamino-propionic acid methyl ester

Guidance literature:: With silver orthophosphate; 1,3-bis-(diphenylphosphino)propane; tetrabutylammomium bromide; Pd₂(dba)3/Pd₂(dba)3*CH₃Cl; In toluene; at 90 - 95 ℃; for 26h;
DOI:10.1039/b609604b