dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate

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Chemical Name:dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate
CAS No.:1101185-56-1
Molecular Formula:C₃₄H₅₈NO₈P
Molecular Weight:639.81
Hs Code.:

Synonyms:dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate

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Technology Process of dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate

There total 1 articles about dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 13360-61-7
1-pentadecene

: 1101185-55-0
dimethyl (3S,4R)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)hex-5-enylphosphonate

: 1101185-56-1
dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 7h; Reflux;
DOI:10.1016/j.tet.2008.10.018

Reference yield: 76.0%

: 1101185-56-1
dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate

: 112-67-4
n-hexadecanoyl chloride

: 1101185-57-2
dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(1-oxohexadecylamino)nonadec-5-enylphosphonate

Guidance literature:: dimethyl (3S,4R,5E)-4-(benzyloxycarbonyloxy)-3-(tert-butyloxycarbonylamino)nonadec-5-enylphosphonate; With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;

n-hexadecanoyl chloride; With potassium carbonate; In dichloromethane; water; at 0 ℃; for 0.25h;
DOI:10.1016/j.tet.2008.10.018