1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt

Base Information

Chemical Name:1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt
CAS No.:852705-14-7
Molecular Formula:CHF₃O₃S*C₁₉H₂₁BrFNO
Molecular Weight:528.363
Hs Code.:

Synonyms:1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt

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Chemical Property of 1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt

Chemical Property:

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Technology Process of 1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt

There total 1 articles about 1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 488148-14-7
(S)-(+)-3-(5-bromo-1-(4-fluorophenyl)-1,3-dihydroisobenzofuran-1-yl)-N,N-dimethylpropan-1-amine

: 1493-13-6
trifluorormethanesulfonic acid

: 852705-14-7
1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt

Guidance literature:: In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.5h;

Reference yield:

: 852705-14-7
1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt

: 544-92-3
copper(I) cyanide

: 128196-01-0
escitalopram

Guidance literature:: 1-[3-(dimethylamino)propyl]-1-(4-fluorophenyl)-5-bromo-1,3-dihydroisobenzofuran trifluoromethanesulfonate salt; copper(I) cyanide; In DMF (N,N-dimethyl-formamide); at 145 - 150 ℃; for 33h;

With ethylenediamine; In DMF (N,N-dimethyl-formamide); water; at 25 - 30 ℃; for 4h; Product distribution / selectivity;