C₄₆H₇₀O₂Si₂

Base Information

Chemical Name:C₄₆H₇₀O₂Si₂
CAS No.:896104-59-9
Molecular Formula:C₄₆H₇₀O₂Si₂
Molecular Weight:711.232
Hs Code.:

C<sub>46</sub>H<sub>70</sub>O<sub>2</sub>Si<sub>2</sub>

Synonyms:C₄₆H₇₀O₂Si₂

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Chemical Property of C₄₆H₇₀O₂Si₂

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Technology Process of C₄₆H₇₀O₂Si₂

There total 20 articles about C₄₆H₇₀O₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 896104-58-8
3-{(1S,5S)-2-[(Z)-3-[(1S,2S,5R)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-5-isopropyl-2-methyl-cyclopentyl]-1-(tert-butyl-diphenyl-silanyloxymethyl)-propenyl]-5-methyl-cyclopent-2-enyl}-propionaldehyde

: 90965-06-3
dimethyl 1-(1-diazo-2-oxopropyl)phosphonate

: 896104-59-9
C₄₆H₇₀O₂Si₂

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃;
DOI:10.1021/jo0604585

Reference yield:

: 896104-51-1
(E)-(2S,3S)-2-[3-(4-Methoxy-benzyloxy)-propyl]-3-methyl-hex-4-enoic acid

: 896104-59-9
C₄₆H₇₀O₂Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 80 percent / MsCl; Et₃N / tetrahydrofuran / 1 h / 0 °C

2.1: 82 percent / tetrahydrofuran / 20 °C

3.1: Grubbs catalyst / CH₂Cl₂ / Heating

4.1: H₂ / Pd/C / ethyl acetate / 2 h

5.1: LHMDS / toluene / 1 h / -78 °C

5.2: tetrahydrofuran / 4 h / -78 - 20 °C

6.1: HSnBu₃; Pd(PPh₃)4 / tetrahydrofuran / 2 h

6.2: 1.18 percent / Pd(PPh₃)4; LiCl; CuCl / dimethylsulfoxide / 37 h / 60 °C

7.1: 87 percent / DIBAL-H / CH₂Cl₂ / -78 - 20 °C

8.1: 93 percent / imidazole / dimethylformamide / 18 h / 20 °C

9.1: 91 percent / catecholborane bromide; 2,6-lutidine / CH₂Cl₂ / 7 h / 0 °C

10.1: 87 percent / Dess-Martin periodinane; 2,6-lutidine / CH₂Cl₂ / 2 h

11.1: 96 percent / K₂CO₃ / methanol / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; Grubbs catalyst first generation; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromocatecholborane; hydrogen; tri-n-butyl-tin hydride; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; methanesulfonyl chloride; triethylamine; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; 6.2: Stille coupling / 10.1: Dess-Martin oxidation;
DOI:10.1021/jo0604585

Reference yield:

: 896104-74-8
(2S,3S,4E)-N-methoxy-2-{3-[(4-methoxybenzyl)oxy]propyl}-N,3-dimethylhex-4-enamide

: 896104-59-9
C₄₆H₇₀O₂Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: 82 percent / tetrahydrofuran / 20 °C

2.1: Grubbs catalyst / CH₂Cl₂ / Heating

3.1: H₂ / Pd/C / ethyl acetate / 2 h

4.1: LHMDS / toluene / 1 h / -78 °C

4.2: tetrahydrofuran / 4 h / -78 - 20 °C

5.1: HSnBu₃; Pd(PPh₃)4 / tetrahydrofuran / 2 h

5.2: 1.18 percent / Pd(PPh₃)4; LiCl; CuCl / dimethylsulfoxide / 37 h / 60 °C

6.1: 87 percent / DIBAL-H / CH₂Cl₂ / -78 - 20 °C

7.1: 93 percent / imidazole / dimethylformamide / 18 h / 20 °C

8.1: 91 percent / catecholborane bromide; 2,6-lutidine / CH₂Cl₂ / 7 h / 0 °C

9.1: 87 percent / Dess-Martin periodinane; 2,6-lutidine / CH₂Cl₂ / 2 h

10.1: 96 percent / K₂CO₃ / methanol / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; Grubbs catalyst first generation; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromocatecholborane; hydrogen; tri-n-butyl-tin hydride; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; 5.2: Stille coupling / 9.1: Dess-Martin oxidation;
DOI:10.1021/jo0604585