N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide

Base Information

Chemical Name:N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide
CAS No.:1415681-32-1
Molecular Formula:C₄₂H₇₃N₃O₅
Molecular Weight:700.059
Hs Code.:

Synonyms:N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide

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Technology Process of N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide

There total 3 articles about N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 15351-28-7
11-aminoundecanoic acid ethyl ester

: 1415681-31-0
3,5-bis-n-decylaminocarbonyl-benzoic acid

: 1415681-32-1
N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In chloroform; for 48h; Inert atmosphere; Cooling with ice;
DOI:10.1002/anie.201204727

Reference yield:

: 2672-58-4
1,3,5-tris-(methoxycarbonyl)benzene

: 1415681-32-1
N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / methanol / 21 h / 85 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

3: triethylamine / chloroform / 24 h / 20 °C / Inert atmosphere

4: lithium hydroxide monohydrate / methanol; water / 48 h / 20 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 48 h / Inert atmosphere; Cooling with ice

With dmap; lithium hydroxide monohydrate; oxalyl dichloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1002/anie.201204727

Reference yield:

: 18263-95-1
3,5-dicarboxylic acid-1-benzoic acid methyl ester

: 1415681-32-1
N-(ethyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

2: triethylamine / chloroform / 24 h / 20 °C / Inert atmosphere

3: lithium hydroxide monohydrate / methanol; water / 48 h / 20 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 48 h / Inert atmosphere; Cooling with ice

With dmap; lithium hydroxide monohydrate; oxalyl dichloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1002/anie.201204727