4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether

Base Information

Chemical Name:4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether
CAS No.:744251-98-7
Molecular Formula:C₂₁H₂₇BrO₅
Molecular Weight:439.346
Hs Code.:

Synonyms:4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether

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Chemical Property of 4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether

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Technology Process of 4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether

There total 1 articles about 4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 31255-26-2
1-bromo-2-{2-[2-(2-bromoethoxy)ethoxy]-ethoxy}ethane

: 103-16-2
4-Benzyloxyphenol

: 744251-98-7
4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether

Guidance literature:: With potassium carbonate; In acetone; for 36h; Heating;
DOI:10.1016/j.tet.2004.05.066

Reference yield: 98.0%

: 744251-98-7
4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether

: 292080-87-6
4-(2-{2-[2-(2-bromoethoxy)ethoxy]ethoxy}ethoxy)phenol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 8h; under 760.051 Torr;
DOI:10.1016/j.tet.2004.05.066 DOI:10.1016/j.tet.2004.06.104

Reference yield:

: 744251-98-7
4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]-phenyl benzyl ether

: 744251-99-8
2-bromo-4-[2-[2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy]-ethoxy]phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / H₂ / Pd-C / ethyl acetate / 8 h / 20 °C / 760.05 Torr

2: 100 percent / Br₂ / CHCl₃ / 1 h / 0 °C

With hydrogen; bromine; palladium on activated charcoal; In chloroform; ethyl acetate;
DOI:10.1016/j.tet.2004.06.104