benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside

Base Information

Chemical Name:benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside
CAS No.:73892-49-6
Molecular Formula:C₂₃H₂₆O₈S
Molecular Weight:462.521
Hs Code.:

Synonyms:benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside

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Technology Process of benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside

There total 2 articles about benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

: 30694-75-8,110550-22-6,110550-23-7
1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-α-D-gluco-hexodialdo-1,4:6,3-difuranose

: 100-39-0
benzyl bromide

: 73892-49-6
benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside

Guidance literature:: With silver(l) oxide; In toluene; for 6h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85313-6

Reference yield:

: 55263-78-0
1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-α-D-glucofuranurono-6,3-lactone

: 73892-49-6
benzyl 1,2-O-isopropylidene-5-O-toluene-p-sulphonyl-(6S)-α-D-gluco-hexodialdo-1,4-furanose-6,3-furanoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / di-isobutyl aluminium hydride

2: 86.5 percent / silver oxide / toluene / 6 h / Ambient temperature

With diisobutylaluminium hydride; silver(l) oxide; In toluene;
DOI:10.1016/S0008-6215(00)85313-6