di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate

Base Information

Chemical Name:di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate
CAS No.:944088-77-1
Molecular Formula:C₂₁H₃₄ClN₄O₁₀P
Molecular Weight:568.949
Hs Code.:

Synonyms:di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate

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Technology Process of di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate

There total 4 articles about di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1072-52-2
2-(1-aziridine)ethanol

: 944088-64-6
di(tert-butyl) 2-[(2-chloro-3,5-dinitrobenzoyl)amino]ethyl phosphate

: 944088-77-1
di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate

Guidance literature:: With triethylamine; In 1,4-dioxane; at 20 ℃;

Reference yield: 90.0%

: 944088-64-6
di(tert-butyl) 2-[(2-chloro-3,5-dinitrobenzoyl)amino]ethyl phosphate

: 2576-29-6
2-[(2-chloroethyl)amino]ethanol hydrochloride

: 944088-77-1
di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate

Guidance literature:: With triethylamine; In 1,4-dioxane; at 20 ℃;
DOI:10.1016/j.tet.2007.04.044

Reference yield:

: 680199-29-5
2-chloro-3,5-dinitro-N-(2-hydroxyethyl)benzamide

: 944088-77-1
di(tert-butyl) 2-({2-[(2-chloroethyl)(2-hydroxyethyl)amino]-3,5-dinitrobenzoyl}amino)ethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-tetrazole / dimethylformamide; tetrahydrofuran / 2 h / 20 °C

1.2: 51 percent / aq. H₂O₂ / dimethylformamide; tetrahydrofuran / 0.5 h / 10 °C

2.1: 90 percent / Et₃N / dioxane / 20 °C

With 1H-tetrazole; triethylamine; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.04.044