3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane

Base Information

Chemical Name:3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane
CAS No.:152492-57-4
Molecular Formula:C₃₃H₄₄O₁₀S₄
Molecular Weight:728.97
Hs Code.:

Synonyms:3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane

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Chemical Property of 3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane

Chemical Property:

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Technology Process of 3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane

There total 2 articles about 3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 623-51-8
ethyl 2-sulfanylacetate

: 147197-47-5
3,5,3',5'-tetrakis(chloromethyl)-4,4'-dihydroxydiphenylmethane

: 152492-57-4
3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 4h;

Reference yield:

: 13653-12-8
4,4'-methylenebis[2,6-bis(hydroxymethyl)phenol]

: 152492-57-4
3,5,3',5'-tetrakis(ethoxycarbonylmethylthiomethyl)-4,4'-dihydroxydiphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / thionyl chloride / CHCl₃ / 72 h / Ambient temperature

2: 50 percent / anhyd. K₂CO₃ / dimethylformamide / 4 h / 60 °C

With thionyl chloride; potassium carbonate; In chloroform; N,N-dimethyl-formamide;