6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione

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Chemical Name:6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione
CAS No.:133549-89-0
Molecular Formula:C₂₇H₂₆N₄O₄S
Molecular Weight:502.594
Hs Code.:

Synonyms:6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione

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Chemical Property of 6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione

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Technology Process of 6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione

There total 3 articles about 6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 133549-84-5
6-Cyclohexyl-2-phenyl-4-phenylsulfanylmethyl-6,7-dihydro-4H-pyrazolo[1,5-a]pyrrolo[3,4-d]pyrimidine-5,8-dione

: 133549-89-0
6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1.5h; Ambient temperature;
DOI:10.1021/jm00109a028

Reference yield:

: 129095-32-5
6-cyclohexyl-4,7-dihydro-2-phenyl-5H-pyrazolo[1,5-a]pyrrolo[3,4-d]pyrimidine-5,8(6H)-dione

: 133549-89-0
6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / tetrabutylammonium fluoride / tetrahydrofuran; dimethylformamide / 19 h / Ambient temperature

2: 65 percent / 80percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

With tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00109a028

Reference yield:

: 4563-90-0
4-Ethoxycarbonyl-1-cyclohexyl-3-hydroxy-3-pyrrolin-2-on

: 133549-89-0
6-cyclohexyl-6,7-dihydro-2-phenyl-4-((phenylsulfonyl)methyl)-4H-pyrazolo<1,5-a>pyrrolo<3,4-d>pyrimidine-5,8-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / glacial acetic acid / Heating

2: 34 percent / tetrabutylammonium fluoride / tetrahydrofuran; dimethylformamide / 19 h / Ambient temperature

3: 65 percent / 80percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

With tetrabutyl ammonium fluoride; acetic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00109a028