Technology Process of C25H23N5O3
There total 8 articles about C25H23N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
DMF (N,N-dimethyl-formamide);
at 70 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / isopropyl alcohol / 2 h / Heating / reflux
2.1: ethylene glycol / 2 h / Heating / reflux
3.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h / 50 °C
3.2: 20 °C
4.1: DMF (N,N-dimethyl-formamide) / 5 h / 70 °C
With
sodium hydride; triethylamine;
In
DMF (N,N-dimethyl-formamide); ethylene glycol; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: acetic acid / 5 h / Heating / reflux
2.1: triethylamine / methanol / 4 h / Heating / reflux
3.1: trichlorophosphate / 1 h / 10 °C
3.2: 1.5 h / 10 - 20 °C
3.3: 60 °C
4.1: triethylamine / isopropyl alcohol / 2 h / Heating / reflux
5.1: ethylene glycol / 2 h / Heating / reflux
6.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h / 50 °C
6.2: 20 °C
7.1: DMF (N,N-dimethyl-formamide) / 5 h / 70 °C
With
sodium hydride; triethylamine; trichlorophosphate;
In
methanol; DMF (N,N-dimethyl-formamide); ethylene glycol; acetic acid; isopropyl alcohol;