tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate

Base Information

• Chemical Name: tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate
• CAS No.: 1236766-59-8
• Molecular Formula: C₃₀H₄₂F₃N₃O₅SSi
• Molecular Weight: 641.827

Synonyms:tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate

Chemical Property of tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate

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Technology Process of tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate

There total 1 articles about tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tert-butyl 4-({4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate (1236766-41-8) + 2-(tert-butyldimethylsilyloxy)ethyl bromide (86864-60-0) → tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate (1236766-59-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

tert-butyl 4-({7-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate (1236766-59-8) → 4-({7-(2-Hydroxyethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoic acid (1236766-60-1)

Guidance literature:

With hydrogenchloride; water; In acetonitrile; at 20 ℃; for 8h;

upstream raw materials:

Tert-butyl 4-({4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoate

2-(tert-butyldimethylsilyloxy)ethyl bromide

Downstream raw materials:

4-({7-(2-Hydroxyethyl)-4-oxo-3-[4-(2,2,2-trifluoroethoxy)phenyl]-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl}sulfanyl)butanoic acid

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