(S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester

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Chemical Name:(S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester
CAS No.:808771-74-6
Molecular Formula:C₃₀H₃₉N₃O₇
Molecular Weight:553.656
Hs Code.:

Synonyms:(S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester

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Chemical Property of (S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester

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Technology Process of (S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester

There total 4 articles about (S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 808771-74-6
(S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium PF₆; ethyldiisopropylamine / CH₂Cl₂

2: 100 percent / trifluoroacetic acid / CH₂Cl₂; methoxybenzene

3: O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium PF₆; ethyldiisopropylamine / CH₂Cl₂

With N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In dichloromethane; methoxybenzene;
DOI:10.1016/j.bmc.2006.03.028

Reference yield:

: 500213-45-6
(S)-2-((S)-1-Methoxycarbonyl-2-phenyl-ethylcarbamoyl)-piperidine-1-carboxylic acid tert-butyl ester

: 808771-74-6
(S)-2-({(S)-1-[(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionyl]-piperidine-2-carbonyl}-amino)-3-phenyl-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / trifluoroacetic acid / CH₂Cl₂; methoxybenzene

2: O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium PF₆; ethyldiisopropylamine / CH₂Cl₂

With N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In dichloromethane; methoxybenzene;
DOI:10.1016/j.bmc.2006.03.028