2,6-dimethyl-α-phenylbenzenemethanol

Base Information

Chemical Name:2,6-dimethyl-α-phenylbenzenemethanol
CAS No.:21945-72-2
Molecular Formula:C₁₅H₁₆O
Molecular Weight:212.291
Hs Code.:

Synonyms:2,6-dimethyl-α-phenylbenzenemethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-dimethyl-α-phenylbenzenemethanol

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Technology Process of 2,6-dimethyl-α-phenylbenzenemethanol

There total 3 articles about 2,6-dimethyl-α-phenylbenzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 6781-98-2
2,6-dimethyl-1-chlorobenzene

: 100-52-7
benzaldehyde

: 21945-72-2
2,6-dimethyl-α-phenylbenzenemethanol

Guidance literature:: 2,6-dimethyl-1-chlorobenzene; With 2-Bromo-m-xylene; iodine; magnesium; In tetrahydrofuran; at 175 ℃; for 1h; microwave irradiation;

benzaldehyde; In tetrahydrofuran; at 100 ℃; for 0.5h; microwave irradiation;
DOI:10.1055/s-2005-869856

Reference yield: 79.0%

: 1123-56-4
2,6-dimethylbenzaldehyde

: 98-80-6
phenylboronic acid

: 21945-72-2
2,6-dimethyl-α-phenylbenzenemethanol

Guidance literature:: With potassium tert-butylate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; tetrakis(trifluoroacetato)rhodium(II); In tert-Amyl alcohol; at 60 ℃; for 1h;
DOI:10.1021/jo800087n

Reference yield: 51.0%

: 576-22-7
2-Bromo-m-xylene

: 100-52-7
benzaldehyde

: 21945-72-2
2,6-dimethyl-α-phenylbenzenemethanol

Guidance literature:: 2-Bromo-m-xylene; With magnesium; In tetrahydrofuran; at 20 ℃; Reflux;

benzaldehyde; In tetrahydrofuran; at 0 - 20 ℃;

With water; sodium carbonate; In tetrahydrofuran;
DOI:10.1021/ol800078j