Technology Process of 1,3-bis(2,6-dimethylphenyl)-3,4,5,6,7,8-hexahydro-1,3-diazocin-1-ium tetrafluoroborate
There total 4 articles about 1,3-bis(2,6-dimethylphenyl)-3,4,5,6,7,8-hexahydro-1,3-diazocin-1-ium tetrafluoroborate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrafluoroborate;
In
water; acetone;
at 20 ℃;
for 0.333333h;
DOI:10.1021/om200467x
- Guidance literature:
-
In
water; acetone;
under Ar; Br-contg. compd. (0.5 mmol) in acetone and B-contg. compd. (0.6 mmol) in H2O were stirred together at room temp. for 20 min; acetone was evapd. at room temp.; the compd. was collected by filtration, dissolved in CH2Cl2 and dried iver MgSO4; after filtration, the solvent was concd. to ca. 2 mL and ether was added to the soln.;
DOI:10.1021/om200467x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / Reflux
2: sodium tetrafluoroborate / water; acetone / 0.33 h / 20 °C
With
sodium tetrafluoroborate; potassium carbonate;
In
water; acetone; acetonitrile;
DOI:10.1021/om200467x
