tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

Base Information

Chemical Name:tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate
CAS No.:1313217-07-0
Molecular Formula:C₃₅H₄₈N₄O₆S
Molecular Weight:652.855
Hs Code.:

Synonyms:tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

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Chemical Property of tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

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Technology Process of tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

There total 7 articles about tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1187450-89-0
tert-butyl (tert-butoxycarbonyl{6-[(pyridin-2-ylsulfonyl)aminomethyl]pyridin-2-yl}amino)acetate

: 1313217-88-7
4-(1-methylpentyl)benzyl alcohol

: 1313217-07-0
tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

Guidance literature:: With tributylphosphine; diamide; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 3006-96-0
3-hydroxymethyl-benzoic acid

: 1313217-07-0
tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.25 h / Cooling with ice

1.2: pH 7.5

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Cooling with ice

2.2: 20 °C / Cooling with ice

3.1: magnesium / tetrahydrofuran / 20 °C / Cooling with ice

4.1: n-butyllithium / hexane; tetrahydrofuran / -70 - 20 °C

4.2: 3 h / 20 °C

5.1: hydrogen / platinum(IV) oxide / ethanol / 6 h / 20 °C / 760.05 Torr

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 16 h / 20 °C

7.1: tributylphosphine; diamide / tetrahydrofuran / 16 h / 20 °C

With n-butyllithium; tributylphosphine; diamide; water; hydrogen; sodium hydride; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; platinum(IV) oxide; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1313217-85-4
1-[4-(4-methoxybenzyloxymethyl)phenyl]pentan-1-one

: 1313217-07-0
tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methylpentyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / -70 - 20 °C

1.2: 3 h / 20 °C

2.1: hydrogen / platinum(IV) oxide / ethanol / 6 h / 20 °C / 760.05 Torr

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 16 h / 20 °C

4.1: tributylphosphine; diamide / tetrahydrofuran / 16 h / 20 °C

With n-butyllithium; tributylphosphine; diamide; water; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; platinum(IV) oxide; In tetrahydrofuran; ethanol; hexane; dichloromethane;