<2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane

Base Information

Chemical Name:<2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane
CAS No.:182323-54-2
Molecular Formula:C₁₇H₂₈NPSe₂
Molecular Weight:435.31
Hs Code.:

Synonyms:<2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane

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Chemical Property of <2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane

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Technology Process of <2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane

There total 1 articles about <2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156995-24-3
(3,5-Di-tert-butyl-2-phosphanyl-benzyl)-dimethyl-amine

: 182323-54-2
<2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane

Guidance literature:: With selenium; 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; at 25 ℃;
DOI:10.1039/c39950000297

Reference yield:

: 182323-54-2
<2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane

: (3,5-di-tert-butyl-2-phosphinothioyl-benzyl)-dimethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur

2: P(NMe₂)3

With sulfur; Hexamethylphosphorous triamide; 1: sulfurization / 2: deselenation;
DOI:10.1080/10426509908546305

Reference yield:

: 182323-54-2
<2,4-di-tert-butyl-6-<(dimethylamino)methyl>phenyl>diselenoxophosphorane

: (3,5-di-tert-butyl-2-phosphoroso-benzyl)-dimethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: MCPBA

2: P(NMe₂)3

With 3-chloro-benzenecarboperoxoic acid; Hexamethylphosphorous triamide; 1: Oxidation / 2: deselenation;
DOI:10.1080/10426509908546305