5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one

Base Information

Chemical Name:5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one
CAS No.:1470364-71-6
Molecular Formula:C₁₆H₁₂Cl₂N₄O
Molecular Weight:347.203
Hs Code.:

Synonyms:5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one

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Chemical Property of 5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one

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Technology Process of 5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one

There total 4 articles about 5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 877315-80-5
3-o-chlorobenzyl-4-amino-4,5-dihydro-1H-1,2,4-triazole-5-one

: 587-04-2
m-Chlorobenzaldehyde

: 1470364-71-6
5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one

Guidance literature:: With acetic acid; at 115 ℃; for 0.0666667h; Time; Microwave irradiation;

Reference yield:

: 2856-63-5
2-Chlorophenylacetonitrile

: 1470364-71-6
5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / diethyl ether

2: 0 - 5 °C

3: hydrazine hydrate / 0.08 h / 125 °C / Microwave irradiation

4: acetic acid / 0.07 h / 115 °C / Microwave irradiation

With hydrogenchloride; hydrazine hydrate; acetic acid; In diethyl ether;

Reference yield:

: 55770-05-3
ethyl o-chlorophenylimidoacetate hydrochloride

: 1470364-71-6
5-(o-chlorobenzyl)-4-m-chlorobenzyliden amino-2,4-dihydro-2H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 0 - 5 °C

2: hydrazine hydrate / 0.08 h / 125 °C / Microwave irradiation

3: acetic acid / 0.07 h / 115 °C / Microwave irradiation

With hydrazine hydrate; acetic acid;