(3-(dodecyloxy)methyl)-3-methylchroman

Base Information

• Chemical Name: (3-(dodecyloxy)methyl)-3-methylchroman
• CAS No.: 1254940-96-9
• Molecular Formula: C₂₃H₃₈O₂
• Molecular Weight: 346.554

Synonyms:(3-(dodecyloxy)methyl)-3-methylchroman

Chemical Property of (3-(dodecyloxy)methyl)-3-methylchroman

Chemical Property:

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Technology Process of (3-(dodecyloxy)methyl)-3-methylchroman

There total 1 articles about (3-(dodecyloxy)methyl)-3-methylchroman which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-Methoxybenzyl bromide (52289-93-7) → (3-(dodecyloxy)methyl)-3-methylchroman (1254940-96-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / Cooling with ice; Inert atmosphere

1.2: 3 h / 85 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 50 °C / Inert atmosphere; Cooling with ice

3.1: hydrogen bromide / 3 h / 140 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / Inert atmosphere; Cooling with ice

4.2: 3 h / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; hydrogen bromide; sodium hydride; In tetrahydrofuran; mineral oil;

DOI:10.1002/hc.20621

upstream raw materials:

o-Methoxybenzyl bromide

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